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FRACTIONAL DISTILLATION OF CRUDE OIL

Saturday, September 26, 2009 § 43



INTRODUCTION

Fractional distillation is the separation of a mixture into its component parts, or fractions, such as in separating chemical compounds by their boiling point by heating them to a temperature at which several fractions of the compound will evaporate. It is a special type of distillation. Generally the component parts boil at less than 25 oC from each other under a pressure of one atmosphere (atm). If the difference in boiling points is greater than 25 oC, a simple distillation is used.

Distillation is the most common form of separation technology used in petroleum refineries, petrochemical and chemical plants and natural gas processing plants. In most cases, the distillation is operated at a continuous steady state. New feed is always being added to the distillation column and products are always being removed. Unless the process is disturbed due to changes in feed, heat, ambient temperature or condensing, the amount of feed being added and the amount of product being removed are normally equal. This is known as continuous, steady state fractional distillation.

Industrial distillation is typically performed in large, vertical cylindrical columns known as “distillation or fractionation towers” or “distillation columns” with diameters ranging from about 65 centimeters to 6 meters and heights ranging from about 6 meters to 60 meters or more. The distillation towers have liquid outlets at intervals up the column which allow for the withdrawal of different fractions or products having different boiling points or boiling ranges. The lightest products (those with the lowest boiling point) exit from the top of the columns and the heaviest products (those with the highest boiling point) exit from the bottom of the column.

For example, fractional distillation is used in oil refineries to separate crude oil into useful substances (or fractions) having different hydrocarbons of different boiling points. The crude oil fractions with higher boiling points:

1. Have more carbon atoms

2. Have higher molecular weights

3. Are darker in color

4. Are more viscous

5. Are more difficult to ignite and to burn

Large-scale industrial towers use reflux to achieve a more complete separation of products. Reflux refers to the portion of the condensed overhead liquid product from a distillation or fractionation tower that is returned to the upper part of the tower. Inside the tower, the reflux liquid flowing downwards provides the cooling needed to condense the vapors flowing upwards, thereby increasing the effectiveness of the distillation tower. The more reflux is provided for a given number of theoretical plates, the better the tower’s separation of lower boiling materials from higher boiling materials. Alternatively, the more reflux provided for a given desired separation, the fewer theoretical plates are required.



p/s: so far, this what have I written for my lab report.. hopefully can finish it by tomorrow..hahaha...

YZYZ, not so gossip boy become science boy..hahah
a

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